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Beilstein J. Org. Chem. 2019, 15, 437–444, doi:10.3762/bjoc.15.38
Graphical Abstract
Scheme 1: Chemical structures of 3a–e and 5a–e, and the cartoon representation of LCST behavior.
Scheme 2: Synthetic routes and yields of 3a–e and 5a–e.
Figure 1: 1H NMR spectra (room temperature) of (a) 5a (5 mg/mL) in CDCl3; (b) 5a (5 mg/mL) in D2O; (c) 3a (5 ...
Figure 2: a) Water solubility of 3a–e and 5a–e at room temperature; b) concentration-dependent LCST behavior ...
Figure 3: Temperature-dependent 1H NMR spectra (400 MHz, D2O) of 3a–c and 5d. Measurement at temperature a) 2...